7O52
CD22 d6-d7 in complex with Fab m971
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08ID-1 |
Synchrotron site | CLSI |
Beamline | 08ID-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-08-26 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1.033200 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 61.478, 119.719, 241.672 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.823 - 2.410 |
Rwork | 0.226 |
R-free | 0.26400 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7o4y |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (v1.14) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 7.531 | 2.550 |
High resolution limit [Å] | 2.410 | 7.150 | 2.410 |
Rmerge | 0.098 | 0.034 | 1.681 |
Rmeas | 0.102 | 0.035 | 1.751 |
Number of reflections | 35031 | 1469 | 5468 |
<I/σ(I)> | 20.19 | 66.81 | 1.46 |
Completeness [%] | 99.6 | 99.3 | 97.4 |
Redundancy | 13.18 | 11.798 | 12.624 |
CC(1/2) | 0.999 | 0.999 | 0.584 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 2M ammonium sulphate, 0.1M HEPES pH 7.5 |