7O38
cytochrome C kustc0562 from Kuenenia stuttgartiensis
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2018-03-01 |
Detector | MAR scanner 345 mm plate |
Wavelength(s) | 1.5418 |
Spacegroup name | P 64 |
Unit cell lengths | 101.650, 101.650, 28.320 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 40.000 - 3.000 |
R-factor | 0.1969 |
Rwork | 0.191 |
R-free | 0.24780 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5mxy |
RMSD bond length | 0.013 |
RMSD bond angle | 1.573 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.020 | 3.100 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.037 | 0.166 |
Rmeas | 0.041 | |
Number of reflections | 3395 | 307 |
<I/σ(I)> | 6.5 | |
Completeness [%] | 95.8 | |
Redundancy | 2.4 | |
CC(1/2) | 0.973 | 0.745 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 293 | 0.2 M NaCl, 30% w/v PEG 8000, 0.1 M imidazole pH 8.0, 0.277 mM cyclohexylethanoyl-N-hydroxyethylglucamide |