7O36
Crystal Structure of SARS-CoV-2 N-CTD in complex with GTP (II)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALBA BEAMLINE XALOC |
Synchrotron site | ALBA |
Beamline | XALOC |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-11-19 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97926 |
Spacegroup name | P 1 |
Unit cell lengths | 43.691, 48.408, 68.668 |
Unit cell angles | 74.37, 89.89, 83.17 |
Refinement procedure
Resolution | 66.090 - 2.000 |
R-factor | 0.1924 |
Rwork | 0.190 |
R-free | 0.24060 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6wzo |
RMSD bond length | 0.015 |
RMSD bond angle | 1.783 |
Data reduction software | XDS |
Data scaling software | Aimless (0.5.31) |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0103) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 66.090 | 66.090 | 2.050 |
High resolution limit [Å] | 2.000 | 8.940 | 2.000 |
Rmerge | 0.082 | 0.057 | 0.315 |
Rmeas | 0.098 | 0.067 | 0.382 |
Rpim | 0.052 | 0.036 | 0.212 |
Total number of observations | 118216 | 1336 | 7766 |
Number of reflections | 34712 | 396 | 2497 |
<I/σ(I)> | 8.9 | 17.6 | 3 |
Completeness [%] | 95.5 | 98.3 | 93.2 |
Redundancy | 3.4 | 3.4 | 3.1 |
CC(1/2) | 0.993 | 0.992 | 0.923 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 4.6 | 294 | 30% PEG 3350 and 0.1 M sodium acetate pH 4.6 |