Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04 |
| Synchrotron site | Diamond |
| Beamline | I04 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2018-10-21 |
| Detector | DECTRIS EIGER2 X 16M |
| Wavelength(s) | 0.9159 |
| Spacegroup name | P 65 2 2 |
| Unit cell lengths | 120.433, 120.433, 115.784 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 77.614 - 3.000 |
| Rwork | 0.222 |
| R-free | 0.26700 |
| Structure solution method | FOURIER SYNTHESIS |
| Starting model (for MR) | 4jvc |
| RMSD bond length | 0.003 |
| RMSD bond angle | 1.302 |
| Data reduction software | DIALS |
| Data scaling software | Aimless |
| Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 104.300 | 3.180 |
| High resolution limit [Å] | 3.000 | 3.000 |
| Number of reflections | 10259 | 1621 |
| <I/σ(I)> | 17.3 | 1.2 |
| Completeness [%] | 99.1 | |
| Redundancy | 18.6 | |
| CC(1/2) | 1.000 | 0.887 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 100 mM Trisodium Citrate 200 mM Ammonium acetate 4-10% MPD |
