Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04 |
| Synchrotron site | Diamond |
| Beamline | I04 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2018-10-21 |
| Detector | DECTRIS EIGER2 X 16M |
| Wavelength(s) | 0.9159 |
| Spacegroup name | P 65 2 2 |
| Unit cell lengths | 119.788, 119.788, 116.499 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 77.470 - 2.650 |
| Rwork | 0.232 |
| R-free | 0.26060 |
| Structure solution method | FOURIER SYNTHESIS |
| Starting model (for MR) | 4jvc |
| RMSD bond length | 0.004 |
| RMSD bond angle | 1.320 |
| Data reduction software | DIALS |
| Data scaling software | Aimless |
| Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 77.590 | 2.780 |
| High resolution limit [Å] | 2.650 | 2.650 |
| Number of reflections | 14874 | 19002 |
| <I/σ(I)> | 10.7 | 2 |
| Completeness [%] | 99.9 | |
| Redundancy | 9.3 | |
| CC(1/2) | 0.806 | 0.676 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 100 mM Trisodium Citrate 200 mM Ammonium acetate 4-10% MPD |
