7O21
Structure of Bdellovibrio bacteriovorus Bd1075
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-02-26 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9795 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 49.189, 100.631, 62.279 |
Unit cell angles | 90.00, 108.07, 90.00 |
Refinement procedure
Resolution | 46.762 - 1.340 |
R-factor | 0.1873 |
Rwork | 0.186 |
R-free | 0.21270 |
Structure solution method | SAD |
Data reduction software | XDS |
Data scaling software | xia2 |
Phasing software | SOLVE |
Refinement software | PHENIX (1.15.2_3472) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 51.010 | 51.050 | 1.360 |
High resolution limit [Å] | 1.340 | 3.640 | 1.340 |
Rmeas | 0.062 | 0.024 | 2.321 |
Rpim | 0.024 | 0.010 | 0.950 |
Total number of observations | 847565 | 41394 | 32389 |
Number of reflections | 123314 | 6521 | 5505 |
<I/σ(I)> | 17.5 | 100 | 0.4 |
Completeness [%] | 95.7 | 99.4 | 85.5 |
Redundancy | 6.9 | 6.3 | 5.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.8 | 291 | 0.1M Tris pH 7.8 0.1M KSCN 0.1M NaBr 35% peg smear broad |