7NZC
First SH3 domain of POSH (Plenty of SH3 Domains protein)
This is a non-PDB format compatible entry.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-08-01 |
Detector | DECTRIS EIGER2 XE 16M |
Wavelength(s) | 0.9795 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 35.962, 35.962, 181.333 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 30.694 - 1.111 |
Rwork | 0.147 |
R-free | 0.17750 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | modified 2SRC |
RMSD bond length | 0.010 |
RMSD bond angle | 1.677 |
Data reduction software | xia2 |
Data scaling software | xia2 |
Phasing software | PHASER |
Refinement software | REFMAC (7.0.078) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.700 | 1.130 |
High resolution limit [Å] | 1.110 | 1.110 |
Number of reflections | 2677 | 404 |
<I/σ(I)> | 26.1 | 1.4 |
Completeness [%] | 96.0 | |
Redundancy | 19.4 | |
CC(1/2) | 0.999 | 0.565 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 8 | 293 | 0.2 M NaF, 22% PEG 3350 |