7NX1

TG domain of LTK

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PETRA III, EMBL c/o DESY BEAMLINE P13 (MX1)
Synchrotron site	PETRA III, EMBL c/o DESY
Beamline	P13 (MX1)
Temperature [K]	100
Detector technology	PIXEL
Collection date	2019-11-27
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.9763
Spacegroup name	P 1 21 1
Unit cell lengths	55.040, 54.460, 55.010
Unit cell angles	90.00, 111.28, 90.00

Refinement procedure

Resolution	51.260 - 1.300
R-factor	0.1598
Rwork	0.159
R-free	0.18050
Structure solution method	SAD
RMSD bond length	0.007
RMSD bond angle	1.097
Data reduction software	XDS
Data scaling software	XDS
Phasing software	AutoSol
Refinement software	PHENIX (1.17.1_3660)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	51.260	1.380
High resolution limit [Å]	1.300	1.300
Rmeas	0.070	1.260
Number of reflections	145183	23510
<I/σ(I)>	11.5
Completeness [%]	99.1
Redundancy	3.4
CC(1/2)	0.990	0.550

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		287	MOPSO/Bis-Tris pH 6.3 12% PEG 20000 25% Trimethyl propane 2% w/v NDSB 195 5mM YCl3 . 6H2O 5mM ErCl3 . 6H2O 5mM TbCl3 . 6H2O 5mM YbCl3 . 6H2O