Experimental procedure
Detector technology | IMAGE PLATE |
Detector | RIGAKU RAXIS |
Wavelength(s) | 1.5418 |
Spacegroup name | I 4 3 2 |
Unit cell lengths | 182.800, 182.800, 182.800 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 6.000 - 2.000 |
R-factor | 0.152 |
Rwork | 0.152 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.790 |
Data reduction software | R-AXIS |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | Outer shell | |
High resolution limit [Å] | 2.000 * | 2.000 * |
Rmerge | 0.012 | 0.175 * |
Number of reflections | 33570 | |
Completeness [%] | 66.0 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion * | 6.6 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 10-15 (mg/ml) | |
2 | 1 | drop | potassium phosphate | 1.7 (M) | |
3 | 1 | reservoir | potassium phosphate | 1.9 (M) |