7NE3
Human TET2 in complex with favourable DNA substrate.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, DESY BEAMLINE P11 |
Synchrotron site | PETRA III, DESY |
Beamline | P11 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-06-22 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 1.033200 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 47.994, 87.711, 260.531 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 43.860 - 2.260 |
R-factor | 0.1775 |
Rwork | 0.175 |
R-free | 0.22630 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4nm6 |
RMSD bond length | 0.008 |
RMSD bond angle | 0.911 |
Data reduction software | XDS |
Data scaling software | XDS |
Refinement software | PHENIX (1.16_3549) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.340 |
High resolution limit [Å] | 2.260 | 2.260 |
Rmerge | 0.129 | 1.571 |
Rmeas | 0.133 | |
Rpim | 0.037 | 0.453 |
Number of reflections | 26450 | 2568 |
<I/σ(I)> | 16.4 | 1.5 |
Completeness [%] | 99.9 | 99.2 |
Redundancy | 13.1 | 12.7 |
CC(1/2) | 0.999 | 0.689 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.3 | 278 | 0.1M MES pH6.3, 23% PEG2000MME |