7NDI
Crystal structure of ZC3H12C PIN domain with Mg2+ Ion
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.1 |
Synchrotron site | BESSY |
Beamline | 14.1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-07-19 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.91841 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 114.701, 114.701, 257.309 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 48.767 - 2.875 |
R-factor | 0.1928 |
Rwork | 0.192 |
R-free | 0.21470 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3v34 |
RMSD bond length | 0.002 |
RMSD bond angle | 0.682 |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.770 | 2.978 |
High resolution limit [Å] | 2.870 | 2.875 |
Number of reflections | 45274 | 4314 |
<I/σ(I)> | 13.44 | |
Completeness [%] | 99.5 | |
Redundancy | 5.77 | |
CC(1/2) | 0.997 | 0.717 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.2 M LiCl, 50 mM MgSO4 and 8% PEG 8000 |