7N2S
AS3.1-PRPF3-HLA*B27
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL12-1 |
Synchrotron site | SSRL |
Beamline | BL12-1 |
Temperature [K] | 80 |
Detector technology | PIXEL |
Collection date | 2020-02-28 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.97946 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 83.211, 52.789, 106.291 |
Unit cell angles | 90.00, 98.28, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.560 | 2.880 |
High resolution limit [Å] | 2.370 | 2.750 |
Number of reflections | 23506 | 2936 |
<I/σ(I)> | 4.9 | |
Completeness [%] | 97.1 | |
Redundancy | 3.4 | |
CC(1/2) | 0.974 | 0.506 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 25% PEG3350 with 0.2M Ammonium tartrate dibasic dihydrate |