7N2J

MicroED structure of a mutant mammalian prion segment phased by ARCIMBOLDO-BORGES

Experimental procedure

Spacegroup name	P 1
Unit cell lengths	4.870, 10.060, 30.660
Unit cell angles	94.85, 90.26, 99.99

Refinement procedure

Resolution	7.980 - 1.500
R-factor	0.1798
Rwork	0.174
R-free	0.22650
Data reduction software	XDS
Data scaling software	XSCALE
Refinement software	PHENIX

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	7.980	7.980	0.920
High resolution limit [Å]	0.900	4.030	0.900
Rmerge	0.197	0.143	0.466
Rmeas	0.214	0.153	0.520
Total number of observations	18502
Number of reflections	915	30	258
<I/σ(I)>	5.21	9.93	2.55
Completeness [%]	81.0	63.8	81.1
Redundancy	5.383	6.833	4.779
CC(1/2)	0.988	0.982	0.813

Crystallization Conditions

crystal ID	method	pH	temperature	details
1