7N27
Crystal Structure of chromodomain of CDYL in complex with inhibitor UNC6261
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-07-29 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.97934 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 62.971, 76.386, 80.628 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.640 - 1.850 |
R-factor | 0.227 |
Rwork | 0.225 |
R-free | 0.26200 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6v41 |
RMSD bond length | 0.014 |
RMSD bond angle | 1.572 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.870 |
High resolution limit [Å] | 1.840 | 1.840 |
Rmerge | 0.083 | 0.752 |
Number of reflections | 33365 | |
<I/σ(I)> | 10.5 | |
Completeness [%] | 99.3 | 98.8 |
Redundancy | 5.9 | 4.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 291 | 3.5M Na Formate, 0.1M Bis-Tris propane pH7.0 |