7MVT
Crystal structure of the Chaetomium thermophilum Nup192-Nic96 complex (Nup192 residues 185-1756; Nic96 residues 187-301)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL12-2 |
Synchrotron site | SSRL |
Beamline | BL12-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-01-08 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.14012 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 76.776, 76.776, 712.505 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 38.570 - 3.600 |
R-factor | 0.261 |
Rwork | 0.258 |
R-free | 0.29670 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5hb4 |
RMSD bond length | 0.002 |
RMSD bond angle | 0.443 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.19.1_4122) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 3.730 |
High resolution limit [Å] | 3.600 | 3.600 |
Rmerge | 0.142 | 1.832 |
Rmeas | 0.146 | 1.882 |
Rpim | 0.032 | 0.416 |
Number of reflections | 46821 | 2539 |
<I/σ(I)> | 12.4 | 1.66 |
Completeness [%] | 99.6 | 97.74 |
Redundancy | 20.8 | 18.9 |
CC(1/2) | 1.000 | 0.778 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 294 | 0.05 M HEPES pH 7.5, 0.1 M ammonium sulfate, 8 % (w/v) PEG 3350, 1 % (v/v) 2-propanol |