7MRO
Zebrafish CNTN4 FN1-FN3 domains
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-04-14 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.0 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 44.700, 56.880, 130.940 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 36.920 - 1.870 |
R-factor | 0.1772 |
Rwork | 0.174 |
R-free | 0.21590 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5e4s |
RMSD bond length | 0.006 |
RMSD bond angle | 0.843 |
Data reduction software | MOSFLM |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 56.880 | 1.910 |
High resolution limit [Å] | 1.870 | 1.870 |
Rmerge | 0.131 | 0.275 |
Rmeas | 0.136 | 0.285 |
Rpim | 0.037 | 0.075 |
Number of reflections | 28351 | 1791 |
<I/σ(I)> | 12.7 | 8.5 |
Completeness [%] | 100.0 | 100 |
Redundancy | 13.2 | 13.9 |
CC(1/2) | 0.994 | 0.978 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 100mM Na-acetate pH 5.5, 30% (w/v) PEG 8,000 |