7MO6
Guanosine Monophosphate Synthase from Aspergillus fumigatus Af293
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2019-03-30 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9537 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 47.297, 159.761, 76.173 |
Unit cell angles | 90.00, 108.00, 90.00 |
Refinement procedure
Resolution | 39.940 - 2.300 |
R-factor | 0.2323 |
Rwork | 0.230 |
R-free | 0.27730 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2ywc |
Data reduction software | XDS (20190315) |
Data scaling software | Aimless (0.6.3) |
Phasing software | PHASER (2.8.3) |
Refinement software | PHENIX (1.16-3549) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 44.940 | 44.940 | 2.380 |
High resolution limit [Å] | 2.300 | 8.910 | 2.300 |
Rmerge | 0.209 | 0.067 | 2.453 |
Rmeas | 0.227 | 0.073 | 2.692 |
Rpim | 0.089 | 0.029 | 1.090 |
Total number of observations | 311610 | 5636 | 27578 |
Number of reflections | 47553 | 854 | 4684 |
<I/σ(I)> | 6.1 | 23 | 0.9 |
Completeness [%] | 99.8 | 99.3 | 100 |
Redundancy | 6.6 | 6.6 | 5.9 |
CC(1/2) | 0.992 | 0.993 | 0.353 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 289.15 | 21% PEG 3350, 0.05 M Bis-Tris pH 6.5 |