7MNE
PTP1B P206G mutation, open state
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL12-2 |
Synchrotron site | SSRL |
Beamline | BL12-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-06-26 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | .97946 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 88.123, 88.123, 72.377 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 38.160 - 1.600 |
R-factor | 0.1639 |
Rwork | 0.163 |
R-free | 0.17610 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5k9v |
RMSD bond length | 0.015 |
RMSD bond angle | 1.494 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX (1.18.2_3874) |
Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 38.160 | 1.620 |
High resolution limit [Å] | 1.600 | 1.600 |
Rmerge | 0.069 | 0.759 |
Number of reflections | 41756 | 1483 |
<I/σ(I)> | 15.5 | 1.8 |
Completeness [%] | 96.4 | |
Redundancy | 8.1 | |
CC(1/2) | 0.996 | 0.520 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | 0.2 M MgCl2, 0.1 M Tris pH 7.8, 17% PEG |