7MLL
Solution structure of Exenatide (exendin-4) in 30-vol% trifluoroethanol using CS-Rosetta
Spectrometer
Experimental method: SOLUTION NMR
| Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
| 1 | Bruker | AVANCE III | 600 |
Experiment
| experiment id | conditions id | solution id | Experiment type |
| 1 | 1 | 1 | 2D 1H-13C HSQC |
| 2 | 1 | 1 | 2D 1H-15N HSQC |
| 3 | 1 | 1 | 2D 1H-13C HSQC TOCSY |
| 4 | 1 | 1 | 2D 1H-15N HSQC TOCSY |
| 5 | 1 | 1 | 2D 1H-13C HMBC (carbonyl selective) |
| 6 | 1 | 1 | 1D 13C APT |
NMR Sample
| conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
| 1 | 5.35 | 1 | 315 |
Conformers
| Conformers Calculated Total Number | 3000 |
| Conformers Submitted Total Number | 5 |
