7MJ6
HLA-A*02:01 bound to Neuroblastoma Derived IGFBPL1 peptide
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.3.1 |
Synchrotron site | ALS |
Beamline | 8.3.1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-04-04 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.11584 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 111.410, 78.980, 60.370 |
Unit cell angles | 90.00, 97.43, 90.00 |
Refinement procedure
Resolution | 64.250 - 1.950 |
R-factor | 0.1596 |
Rwork | 0.158 |
R-free | 0.19610 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5c07 |
RMSD bond length | 0.007 |
RMSD bond angle | 0.785 |
Data reduction software | MOSFLM |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.13_2998) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 64.250 | 2.000 |
High resolution limit [Å] | 1.950 | 1.950 |
Rmerge | 0.135 | 1.000 |
Number of reflections | 37547 | 2616 |
<I/σ(I)> | 9 | 2.4 |
Completeness [%] | 99.2 | |
Redundancy | 6.1 | |
CC(1/2) | 0.990 | 0.820 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 295 | 1M Sodium Citrate Dibasic, 0.1M Sodium Cacodylate pH 6.5 |