7M1O
Hydrogenobacter thermophilus ferredoxin 1 S64A variant
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | BRUKER AXS MICROSTAR |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-11-22 |
Detector | Bruker Platinum 135 |
Wavelength(s) | 1.54 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 39.635, 69.103, 95.788 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 36.624 - 1.984 |
R-factor | 0.189498381145 |
Rwork | 0.186 |
R-free | 0.21894 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1iqz |
RMSD bond length | 0.005 |
RMSD bond angle | 1.125 |
Data reduction software | PROTEUM PLUS |
Data scaling software | PROTEUM PLUS |
Phasing software | PHENIX |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 56.230 | 2.060 |
High resolution limit [Å] | 1.980 | 1.980 |
Number of reflections | 17128 | 1338 |
<I/σ(I)> | 6 | |
Completeness [%] | 97.3 | |
Redundancy | 2.7 | |
CC(1/2) | 0.991 | 0.652 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 289 | 80% saturated ammonium sulfate, 0.1 M MES (pH 6.5) |