7LYU
Reelin repeat 8
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX1 |
Synchrotron site | Australian Synchrotron |
Beamline | MX1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-09-30 |
Detector | DECTRIS EIGER2 X 9M |
Wavelength(s) | 0.953724 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 60.171, 104.059, 67.615 |
Unit cell angles | 90.00, 104.11, 90.00 |
Refinement procedure
Resolution | 45.120 - 3.000 |
R-factor | 0.229 |
Rwork | 0.227 |
R-free | 0.26350 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2e26 |
RMSD bond length | 0.005 |
RMSD bond angle | 0.895 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | MrBUMP |
Refinement software | PHENIX (1.19.1_4122) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.120 | 3.180 |
High resolution limit [Å] | 3.000 | 3.000 |
Number of reflections | 16263 | 2620 |
<I/σ(I)> | 5.5 | 1.3 |
Completeness [%] | 99.9 | |
Redundancy | 3.6 | |
CC(1/2) | 0.985 | 0.496 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 293 | 0.1M Tris pH 8, 35% PEG 1000 |