7LXG
Homocitrullinated beta-lactamase OXA-48
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08ID-1 |
Synchrotron site | CLSI |
Beamline | 08ID-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-06-28 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1.00 |
Spacegroup name | P 62 |
Unit cell lengths | 143.960, 143.960, 56.030 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 47.122 - 2.200 |
R-factor | 0.1702 |
Rwork | 0.168 |
R-free | 0.21710 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4s2p |
Data reduction software | MOSFLM |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.122 | 2.279 |
High resolution limit [Å] | 2.200 | 2.200 |
Number of reflections | 33900 | 3340 |
<I/σ(I)> | 25.08 | |
Completeness [%] | 99.7 | |
Redundancy | 10.1 | |
CC(1/2) | 1.000 | 0.941 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 298.15 | 0.2M lithium sulphate, 0.1M BIS-Tris pH 5.5, 25% w/v PEG 3350 |