7LOZ
S-adenosylmethionine synthetase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-08-28 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9537 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 122.600, 122.600, 288.835 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 39.090 - 2.250 |
R-factor | 0.1906 |
Rwork | 0.190 |
R-free | 0.21110 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1pl7 |
RMSD bond length | 0.006 |
RMSD bond angle | 0.795 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.750 | 2.310 |
High resolution limit [Å] | 2.250 | 2.250 |
Number of reflections | 61889 | 4507 |
<I/σ(I)> | 14.2 | |
Completeness [%] | 100.0 | |
Redundancy | 30.3 | |
CC(1/2) | 0.998 | 0.549 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293.15 | Bis-Tris 6.5, 15% ethylene glycol, PEG 3350 20% |