7LOW
S-adenosylmethionine synthetase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-08-28 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9537 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 122.954, 122.954, 288.087 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 39.100 - 2.390 |
R-factor | 0.184 |
Rwork | 0.182 |
R-free | 0.21650 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1pl7 |
RMSD bond length | 0.003 |
RMSD bond angle | 0.604 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | MOLREP |
Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.860 | 2.460 |
High resolution limit [Å] | 2.390 | 2.390 |
Number of reflections | 51892 | 4416 |
<I/σ(I)> | 15.5 | |
Completeness [%] | 100.0 | |
Redundancy | 39.4 | |
CC(1/2) | 0.999 | 0.434 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293.15 | 0.1 M Bis-Tris pH 6.5, 15% ethylene glycol, 20% PEG 3350 |