7L6G
MbnP from Methylosinus trichosporium
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-D |
Synchrotron site | APS |
Beamline | 21-ID-D |
Temperature [K] | 77 |
Detector technology | PIXEL |
Collection date | 2020-02-05 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 1.377 |
Spacegroup name | P 61 |
Unit cell lengths | 91.276, 91.276, 383.567 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 21.890 - 2.040 |
R-factor | 0.2067 |
Rwork | 0.204 |
R-free | 0.25100 |
Structure solution method | SAD |
Data reduction software | xia2 |
Data scaling software | xia2 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 77.450 | 77.450 | 2.070 |
High resolution limit [Å] | 2.040 | 11.170 | 2.040 |
Rmerge | 0.348 | 0.086 | 9.169 |
Rmeas | 0.353 | 0.087 | 9.450 |
Rpim | 0.052 | 0.011 | 2.241 |
Total number of observations | 45930 | 83081 | |
Number of reflections | 112407 | 735 | 4848 |
<I/σ(I)> | 13.91 | 35.5 | 1.6 |
Completeness [%] | 98.4 | 99.8 | 84.7 |
Redundancy | 50.6 | 62.5 | 17.1 |
CC(1/2) | 0.990 | 0.997 | 0.379 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | 0.2 M lithium chloride, 1.6 M ammonium sulfate |