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7L68

C-type carbohydrate-recognition domain 4 of the mannose receptor

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSSRL BEAMLINE BL12-1
Synchrotron siteSSRL
BeamlineBL12-1
Temperature [K]100
Detector technologyPIXEL
Collection date2020-09-12
DetectorDECTRIS EIGER X 16M
Wavelength(s)0.97946
Spacegroup nameP 1 21 1
Unit cell lengths31.623, 58.718, 62.383
Unit cell angles90.00, 97.66, 90.00
Refinement procedure
Resolution31.340 - 1.400
R-factor0.1558
Rwork0.155
R-free0.17490
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)7jub
Data reduction softwareXDS
Data scaling softwareAimless (0.7.4)
Refinement softwarePHENIX (1.18.2)
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]31.34031.3401.420
High resolution limit [Å]1.4007.6701.400
Rmerge0.0570.0820.111
Rmeas0.0610.0920.120
Rpim0.0220.0380.044
Total number of observations309250187714754
Number of reflections420222842009
<I/σ(I)>23.632.412.4
Completeness [%]94.497.992.6
Redundancy7.46.67.3
CC(1/2)0.9970.9720.990
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP295Protein solution: 6mg/ml protein in 5mM CaCl2, 10mM Tris, pH 8.0, 25mM NaCl, and 10mM Man9GlcNAc2. Reservoir solution: 2.5% Peg 8K, 0.1M MES, pH 6.0

222036

PDB entries from 2024-07-03

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