7L26
HPK1 IN COMPLEX WITH COMPOUND 38
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-05-03 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.00002 |
Spacegroup name | P 1 |
Unit cell lengths | 58.138, 58.168, 98.955 |
Unit cell angles | 89.84, 90.13, 97.60 |
Refinement procedure
Resolution | 98.950 - 2.300 |
R-factor | 0.2627 |
Rwork | 0.262 |
R-free | 0.29830 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PREVIOUSLY SOLVED STUCTURE |
RMSD bond length | 0.013 |
RMSD bond angle | 1.666 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Refinement software | REFMAC (5.8.0155) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 98.950 | 2.550 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmeas | 0.092 | 0.568 |
Number of reflections | 54548 | 14634 |
<I/σ(I)> | 8.65 | 2.56 |
Completeness [%] | 95.0 | 95.4 |
Redundancy | 2.2 | 2.2 |
CC(1/2) | 0.997 | 0.998 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 293 | UNDISCLOSED |