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7KC8

Salivary protein from Culex quinquefasciatus that belongs to the Cysteins and Tryptophan-Rich (CWRC) family

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU MICROMAX-007
Temperature [K]95
Detector technologyCCD
Collection date2020-02-26
DetectorRIGAKU SATURN A200
Wavelength(s)1.541800
Spacegroup nameP 21 21 21
Unit cell lengths72.940, 73.050, 106.960
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution26.740 - 2.300
R-factor0.2087
Rwork0.205
R-free0.25470
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)homology
Data reduction softwareXDS
Data scaling softwareXSCALE
Phasing softwarePHENIX
Refinement softwarePHENIX (1.18.2_3874)
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]26.74026.7402.360
High resolution limit [Å]2.30010.2902.300
Rmerge0.0310.0210.201
Rmeas0.0320.0220.215
Number of reflections250083311367
<I/σ(I)>59.38103.538.92
Completeness [%]96.197.171.8
Redundancy11.4589.4177.963
CC(1/2)1.0001.0000.969
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP2980.2M Sodium acetate trihydrate, 0.1M TRIS hydrochloride pH 8.5, 30% w/v PEG 4000

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