7K9D
Crystal structure of Bacillus halodurans OapB in complex with its OLE RNA target (crystal form I)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-07-31 |
Detector | DECTRIS EIGER2 X 16M |
Wavelength(s) | 1.6058 |
Spacegroup name | H 3 2 |
Unit cell lengths | 98.817, 98.817, 198.897 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 41.832 - 2.098 |
R-factor | 0.1636 |
Rwork | 0.162 |
R-free | 0.19830 |
Structure solution method | SAD |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | AutoSol |
Refinement software | PHENIX (1.16_3549) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.840 | 2.180 |
High resolution limit [Å] | 2.098 | 2.098 |
Rmerge | 0.050 | 1.211 |
Rmeas | 0.053 | 1.280 |
Rpim | 0.017 | 0.411 |
Number of reflections | 42266 | 2175 |
<I/σ(I)> | 29.9 | 1.7 |
Completeness [%] | 99.9 | 100 |
Redundancy | 9.8 | 9.4 |
CC(1/2) | 0.994 | 0.816 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 292 | 100 mM HEPES (pH 7.0 to 7.5), 200 mM NH4Cl and 39 to 42.5% 2-Methyl-2,4-pentanediol (MPD) |