7K7F
Solution Structure of the Corynebacterium diphtheriae SpaA Pilin-Signal Peptide Complex
Spectrometer
Experimental method: SOLUTION NMR
| Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
| 1 | Bruker | AVANCE III HD | 600 | |
| 2 | Bruker | AVANCE NEO | 800 |
Experiment
| experiment id | conditions id | solution id | Experiment type |
| 1 | 1 | 1 | 3D_15N-separated_NOESY |
| 10 | 1 | 1 | T1/R1 relaxation |
| 11 | 1 | 1 | 3D HN(CA)CO |
| 12 | 1 | 1 | 3D HNCA |
| 13 | 1 | 1 | 3D HNCO |
| 14 | 2 | 2 | 3D HCCH-COSY |
| 17 | 1 | 1 | 3D HNHA |
| 18 | 1 | 1 | 3D HBHA(CO)NH |
| 19 | 1 | 1 | 3D 1H-15N TOCSY |
| 2 | 2 | 1 | 3D_(F1)_13C,15N-filtered_(F2)_15N-edited NOESY-HSQC |
| 20 | 1 | 1 | 3D H(CCO)NH |
| 21 | 2 | 2 | 2D (F1,F2) 13C-filtered NOESY |
| 22 | 2 | 2 | 2D (F1) 13C,15N-filtered TOCSY |
| 23 | 1 | 2 | 3D_(F1)_13C,15N-filtered_(F2)_13C-edited NOESY-HSQC |
| 24 | 2 | 2 | 3D_13C-separated_NOESY_aliphatic_D2O |
| 25 | 1 | 2 | 3D_13C-separated_NOESY_aromatic_D2O |
| 26 | 1 | 1 | 3D_13C-separated_NOESY_aliphatic_H2O |
| 3 | 1 | 1 | 2D 1H-15N HSQC |
| 4 | 2 | 2 | 2D 1H-13C HSQC |
| 5 | 2 | 2 | 2D 1H-13C HSQC aromatic |
| 6 | 1 | 1 | 3D HNCACB |
| 7 | 1 | 1 | 1H-15N heteronoe |
| 8 | 1 | 1 | 3D CBCA(CO)NH |
| 9 | 1 | 1 | T2/R2 relaxation |
NMR Sample
| conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
| 1 | 6 | ambient | 298 |
| 2 | 6 | ambient | 298 |
Conformers
| Conformers Calculated Total Number | 200 |
| Conformers Submitted Total Number | 20 |
