7JTB
CRYSTAL STRUCTURE OF NATIVE BOVINE ARRESTIN 1 IN COMPLEX WITH INOSITOL HEXAKISPHOSPHATE
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-10-25 |
Detector | DECTRIS EIGER2 X 16M |
Wavelength(s) | 0.97920 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 167.300, 187.899, 90.378 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.200 - 2.600 |
R-factor | 0.2064 |
Rwork | 0.205 |
R-free | 0.23830 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.005 |
RMSD bond angle | 1.347 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | REFMAC |
Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.760 |
High resolution limit [Å] | 2.600 | 2.600 |
Rmerge | 0.136 | 2.233 |
Number of reflections | 88202 | 14017 |
<I/σ(I)> | 13.92 | |
Completeness [%] | 99.8 | 99.4 |
Redundancy | 13.1 | |
CC(1/2) | 0.999 | 0.625 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 281 | 0.1 M Bis-Tris propane, 35% 2-Ethoxyethanol, 0.001 M Magnesium acetate, 0.0009 M Phytic acid sodium salt |