7JQS
Abeta 16-36 beta-hairpin mimic with E22delta Osaka mutation
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 123.15 |
Detector technology | CCD |
Collection date | 2017-02-21 |
Detector | RIGAKU SATURN 944+ |
Wavelength(s) | 1.54 |
Spacegroup name | P 41 3 2 |
Unit cell lengths | 47.238, 47.238, 47.238 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 21.126 - 2.127 |
R-factor | 0.2392 |
Rwork | 0.234 |
R-free | 0.28690 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7jqr |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.13_2998) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 21.130 | 2.203 |
High resolution limit [Å] | 2.127 | 2.127 |
Rmerge | 0.004 | 0.027 |
Number of reflections | 1928 | 110 |
<I/σ(I)> | 52.34 | |
Completeness [%] | 99.8 | |
Redundancy | 156.1 | |
CC(1/2) | 1.000 | 0.998 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 297.15 | calcium chloride, sodium acetate, isopropanol |