7JQR
Abeta 16-36 beta-hairpin mimic with E22G Arctic mutation
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 123.15 |
Detector technology | CCD |
Collection date | 2017-10-13 |
Detector | RIGAKU SATURN 944+ |
Wavelength(s) | 1.54 |
Spacegroup name | P 41 3 2 |
Unit cell lengths | 47.219, 47.219, 47.219 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.280 - 2.070 |
R-factor | 0.208 |
Rwork | 0.203 |
R-free | 0.25410 |
Structure solution method | SAD |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHENIX |
Refinement software | PHENIX (dev_3908) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.280 | 2.149 |
High resolution limit [Å] | 2.070 | 2.075 |
Rmerge | 0.012 | |
Rmeas | 0.017 | |
Number of reflections | 2070 | 126 |
<I/σ(I)> | 65.87 | |
Completeness [%] | 99.4 | 100 |
Redundancy | 90.7 | |
CC(1/2) | 1.000 | 0.999 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 297.15 | calcium chloride, sodium acetate, isopropanol |