7JJN
Eubacterium rectale Amy13B (EUR_01860)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-D |
Synchrotron site | APS |
Beamline | 21-ID-D |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-11-13 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 0.979 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 84.180, 82.760, 85.860 |
Unit cell angles | 90.00, 92.86, 90.00 |
Refinement procedure
Resolution | 38.070 - 2.250 |
R-factor | 0.1639 |
Rwork | 0.162 |
R-free | 0.19840 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1wza |
RMSD bond length | 0.006 |
RMSD bond angle | 1.108 |
Data reduction software | xia2 |
Data scaling software | xia2 |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0230) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 38.070 | 2.330 |
High resolution limit [Å] | 2.250 | 2.250 |
Rmerge | 0.150 | 0.840 |
Rmeas | 0.160 | |
Number of reflections | 55448 | 5536 |
<I/σ(I)> | 9.9 | |
Completeness [%] | 99.0 | 99.5 |
Redundancy | 7 | 7.2 |
CC(1/2) | 0.990 | 0.770 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 295 | 0.17M Am Sulfate, 25.5% PEG 4000, 15% glycerol (JCSG+ screen, Molecular Dimensions) |