7JGT
Crystal Structure of FN3tt
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-05-18 |
Detector | RIGAKU SATURN 944 |
Wavelength(s) | 1.5418 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 38.530, 38.530, 105.460 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 31.110 - 1.900 |
R-factor | 0.1826 |
Rwork | 0.177 |
R-free | 0.23350 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | Rosetta generated |
Data reduction software | DENZO |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.18_3855) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 31.110 | 31.110 | 1.950 |
High resolution limit [Å] | 1.900 | 8.500 | 1.900 |
Rmerge | 0.064 | 0.039 | 0.322 |
Rmeas | 0.065 | 0.040 | 0.333 |
Total number of observations | 161213 | ||
Number of reflections | 6681 | 105 | 400 |
<I/σ(I)> | 38.63 | 71.28 | 8.85 |
Completeness [%] | 98.3 | 99.1 | 79.7 |
Redundancy | 24.13 | 18.524 | 14.538 |
CC(1/2) | 1.000 | 0.999 | 0.965 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7.5 | 298 | 0.1 M MES pH 6.5, 28% PEG 3350 |