7HMT
PanDDA analysis group deposition -- Crystal Structure of TRIM21 in complex with Z2004563941
This is a non-PDB format compatible entry.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04-1 |
| Synchrotron site | Diamond |
| Beamline | I04-1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2024-05-24 |
| Detector | DECTRIS EIGER2 XE 9M |
| Wavelength(s) | 0.92124 |
| Spacegroup name | I 4 |
| Unit cell lengths | 95.687, 95.687, 45.749 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 67.660 - 1.280 |
| R-factor | 0.1856 |
| Rwork | 0.185 |
| R-free | 0.20560 |
| Structure solution method | FOURIER SYNTHESIS |
| RMSD bond length | 0.011 |
| RMSD bond angle | 2.010 |
| Data reduction software | XDS |
| Data scaling software | Aimless (0.7.7) |
| Phasing software | REFMAC |
| Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
| Overall | Inner shell | Outer shell | |
| Low resolution limit [Å] | 67.640 | 67.640 | 1.300 |
| High resolution limit [Å] | 1.280 | 7.010 | 1.280 |
| Rmerge | 0.110 | 0.064 | 1.889 |
| Rmeas | 0.115 | 0.066 | 2.084 |
| Rpim | 0.032 | 0.019 | 0.850 |
| Total number of observations | 573429 | 4458 | 7718 |
| Number of reflections | 48980 | 357 | 1371 |
| <I/σ(I)> | 12 | 66.2 | 0.4 |
| Completeness [%] | 91.9 | 99.9 | 52.4 |
| Redundancy | 11.7 | 12.5 | 5.6 |
| CC(1/2) | 0.997 | 0.997 | 0.298 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 8 | 293 | 4 % PEG 400, 2 M AmmSO4, 0.1 M HEPES pH 8 |
