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7GWR

Crystal Structure of B-cell lymphoma 6 protein BTB domain in complex with ligand 6 at 14.76 MGy X-ray dose.

This is a non-PDB format compatible entry.
Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsDIAMOND BEAMLINE I24
Synchrotron siteDiamond
BeamlineI24
Temperature [K]100
Detector technologyPIXEL
Collection date2017-07-31
DetectorDECTRIS PILATUS3 6M
Wavelength(s)0.9686
Spacegroup nameP 61 2 2
Unit cell lengths67.870, 67.870, 167.370
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution34.090 - 1.900
R-factor0.184
Rwork0.183
R-free0.20300
Structure solution methodFOURIER SYNTHESIS
RMSD bond length0.010
RMSD bond angle0.950
Data scaling softwareAimless (0.5.32)
Phasing softwareBUSTER (2.10.3)
Refinement softwareBUSTER (2.10.3)
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]34.09034.0901.940
High resolution limit [Å]1.9009.1101.900
Rmerge0.1040.0451.481
Rmeas0.1100.0481.571
Rpim0.0350.0170.507
Total number of observations168872150210924
Number of reflections182952081159
<I/σ(I)>9.830.31.4
Completeness [%]98.394.199.4
Redundancy9.27.29.4
CC(1/2)0.9970.9980.625
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP72911.0 M K2HPO4, 0.7 M NaH2PO4, 75 mM sodium acetate pH 4.5, 2% DMSO

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