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7GW0

Crystal Structure of B-cell lymphoma 6 protein BTB domain in complex with ligand 4 at 21.00 MGy X-ray dose

This is a non-PDB format compatible entry.
Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsDIAMOND BEAMLINE I24
Synchrotron siteDiamond
BeamlineI24
Temperature [K]100
Detector technologyPIXEL
Collection date2017-07-31
DetectorDECTRIS PILATUS3 6M
Wavelength(s)0.9686
Spacegroup nameP 61 2 2
Unit cell lengths67.860, 67.860, 167.230
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution34.070 - 1.900
R-factor0.194
Rwork0.193
R-free0.21200
Structure solution methodFOURIER SYNTHESIS
RMSD bond length0.009
RMSD bond angle0.960
Data scaling softwareAimless (0.5.32)
Phasing softwareBUSTER (2.10.3)
Refinement softwareBUSTER (2.10.3)
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]34.07034.0701.940
High resolution limit [Å]1.9009.1101.900
Rmerge0.0840.0201.412
Rmeas0.0890.0221.494
Rpim0.0300.0080.483
Total number of observations169296148510983
Number of reflections188242361170
<I/σ(I)>1246.71.4
Completeness [%]100.098.8100
Redundancy96.39.4
CC(1/2)0.9991.0000.752
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP72911.0 M K2HPO4, 0.7 M NaH2PO4, 75 mM sodium acetate pH 4.5, 2% DMSO

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