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7GVH

Crystal Structure of B-cell lymphoma 6 protein BTB domain in complex with ligand 3 at 15.95 MGy X-ray dose

This is a non-PDB format compatible entry.
Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsDIAMOND BEAMLINE I24
Synchrotron siteDiamond
BeamlineI24
Temperature [K]100
Detector technologyPIXEL
Collection date2017-07-31
DetectorDECTRIS PILATUS3 6M
Wavelength(s)0.9686
Spacegroup nameP 61 2 2
Unit cell lengths67.640, 67.640, 166.570
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution33.940 - 1.850
R-factor0.181
Rwork0.180
R-free0.20200
Structure solution methodFOURIER SYNTHESIS
RMSD bond length0.010
RMSD bond angle0.890
Data scaling softwareAimless (0.5.32)
Phasing softwareBUSTER (2.10.3)
Refinement softwareBUSTER (2.10.3)
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]33.94033.9401.890
High resolution limit [Å]1.8509.0601.850
Rmerge0.0970.0401.543
Rmeas0.1030.0431.631
Rpim0.0340.0160.521
Total number of observations180496151011240
Number of reflections198702131221
<I/σ(I)>10.932.81.4
Completeness [%]99.495.7100
Redundancy9.17.19.2
CC(1/2)0.9980.9980.650
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP72911.0 M K2HPO4, 0.7 M NaH2PO4, 75 mM sodium acetate pH 4.5, 2% DMSO

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