7G9A
ARHGEF2 PanDDA analysis group deposition -- ARHGEF2 and RhoA in complex with PCM-0102113-001
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | DIAMOND |
Beamline | I04-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2023-03-02 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.92124 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 70.701, 70.701, 195.581 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 23.400 - 2.583 |
R-factor | 0.2114 |
Rwork | 0.207 |
R-free | 0.29500 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 8bnt |
RMSD bond length | 0.007 |
RMSD bond angle | 0.890 |
Data reduction software | XDS |
Data scaling software | Aimless (0.7.9) |
Phasing software | REFMAC |
Refinement software | BUSTER (2.10.4 (17-FEB-2023)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 66.490 | 66.490 | 2.720 |
High resolution limit [Å] | 2.580 | 8.170 | 2.580 |
Rmerge | 3.229 | 0.096 | |
Rmeas | 3.325 | 0.099 | 61.377 |
Rpim | 0.781 | 0.026 | 14.466 |
Total number of observations | 288016 | 8596 | 42110 |
Number of reflections | 16423 | ||
<I/σ(I)> | 4.6 | 15.4 | 0.6 |
Completeness [%] | 100.0 | 100 | 100 |
Redundancy | 17.5 | 13.5 | 18 |
CC(1/2) | 0.776 | 0.997 | 0.542 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 293 | 100 mM Tris, 2.6M sodium formate |