7G97
ARHGEF2 PanDDA analysis group deposition -- ARHGEF2 and RhoA in complex with Z57899718
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | Diamond |
Beamline | I04-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2023-03-02 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.92124 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 71.226, 71.226, 196.058 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 66.940 - 2.300 |
R-factor | 0.1928 |
Rwork | 0.190 |
R-free | 0.24900 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 8bnt |
RMSD bond length | 0.008 |
RMSD bond angle | 1.566 |
Data reduction software | XDS |
Data scaling software | Aimless (0.7.9) |
Phasing software | REFMAC |
Refinement software | REFMAC (5.8.0405) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 71.270 | 71.270 | 2.380 |
High resolution limit [Å] | 2.300 | 8.910 | 2.300 |
Rmerge | 0.636 | 0.082 | 5.282 |
Rmeas | 0.666 | 0.086 | 5.498 |
Rpim | 0.143 | 0.021 | 1.180 |
Total number of observations | 491371 | 7865 | 47958 |
Number of reflections | 23427 | ||
<I/σ(I)> | 6.1 | 16.5 | 1.3 |
Completeness [%] | 100.0 | 100 | 100 |
Redundancy | 21 | 15.5 | 21.4 |
CC(1/2) | 0.992 | 0.998 | 0.629 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 293 | 100 mM Tris, 2.6M sodium formate |