7G8N
ARHGEF2 PanDDA analysis group deposition -- ARHGEF2 and RhoA in complex with Z1262549981
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | Diamond |
Beamline | I04-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-11-25 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.92124 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 71.301, 71.301, 196.090 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 35.150 - 2.320 |
R-factor | 0.2178 |
Rwork | 0.214 |
R-free | 0.28290 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 8bnt |
RMSD bond length | 0.007 |
RMSD bond angle | 0.890 |
Data reduction software | XDS |
Data scaling software | Aimless (0.7.7) |
Phasing software | REFMAC |
Refinement software | BUSTER (2.10.4 (17-FEB-2023)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 35.150 | 35.150 | 2.400 |
High resolution limit [Å] | 2.320 | 8.990 | 2.320 |
Rmerge | 0.694 | 0.111 | 5.273 |
Rmeas | 0.707 | 0.114 | 5.374 |
Rpim | 0.137 | 0.025 | 1.032 |
Total number of observations | 592913 | 9596 | 58029 |
Number of reflections | 22854 | ||
<I/σ(I)> | 4.9 | 22.8 | 0.7 |
Completeness [%] | 100.0 | 98.8 | 99.9 |
Redundancy | 25.9 | 20 | 26.5 |
CC(1/2) | 0.987 | 0.998 | 0.343 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 293 | 100 mM Tris, 2.6M sodium formate |