7FLX
PanDDA analysis group deposition -- Aar2/RNaseH in complex with fragment P05G08 from the F2X-Universal Library
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | MAX IV BEAMLINE BioMAX |
Synchrotron site | MAX IV |
Beamline | BioMAX |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-05-15 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.999900 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 89.279, 81.957, 93.489 |
Unit cell angles | 90.00, 108.25, 90.00 |
Refinement procedure
Resolution | 44.390 - 1.750 |
R-factor | 0.2568 |
Rwork | 0.256 |
R-free | 0.28750 |
Structure solution method | FOURIER SYNTHESIS |
Data reduction software | XDS (Jan 10, 2022) |
Data scaling software | Aimless |
Phasing software | PHENIX (1.17.1_3660) |
Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 44.390 | 44.390 | 44.390 |
High resolution limit [Å] | 1.750 | 5.230 | 1.750 |
Rmerge | 0.037 | 2.663 | |
Rmeas | 0.069 | 0.040 | 2.893 |
Total number of observations | 433691 | 16969 | 64855 |
Number of reflections | 63735 | 2489 | 9930 |
<I/σ(I)> | 12.23 | 44.15 | 0.59 |
Completeness [%] | 99.2 | 99.5 | 96 |
Redundancy | 6.8 | 6.82 | 6.53 |
CC(1/2) | 0.999 | 0.999 | 0.287 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 293 | 19% PEG4000, 3% DMSO, 0.1 M Tris, pH 8.5, 0.2 M lithium sulfate |