7FIA
Structure of AcrIF23
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-07-20 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.979 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 65.569, 65.569, 95.053 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 32.780 - 2.130 |
R-factor | 0.2065 |
Rwork | 0.205 |
R-free | 0.23130 |
Structure solution method | SAD |
Data reduction software | HKL-3000 |
Data scaling software | SCALEPACK |
Phasing software | AutoSol |
Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.210 |
High resolution limit [Å] | 2.130 | 2.130 |
Rmerge | 0.104 | 0.702 |
Number of reflections | 12158 | 1180 |
<I/σ(I)> | 34.8 | |
Completeness [%] | 99.9 | |
Redundancy | 24.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 293 | Sodium fluoride |