7FGA
Alpha-1,2-glucosyltransferase_UDP_sucrose_tll1591
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-10-21 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97930 |
Spacegroup name | P 65 |
Unit cell lengths | 157.712, 157.712, 187.803 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 19.960 - 3.200 |
R-factor | 0.2939 |
Rwork | 0.292 |
R-free | 0.32720 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7fg9 |
Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.960 | 3.370 |
High resolution limit [Å] | 3.200 | 3.200 |
Rmerge | 0.190 | 0.990 |
Number of reflections | 43413 | 6364 |
<I/σ(I)> | 6.3 | |
Completeness [%] | 99.4 | |
Redundancy | 5.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | ammonium sulfate |