7FFS

Human Serum Albumin_1

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL18U1
Synchrotron site	SSRF
Beamline	BL18U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2021-07-12
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.97915
Spacegroup name	P 1 21 1
Unit cell lengths	55.587, 87.123, 58.861
Unit cell angles	90.00, 103.67, 90.00

Refinement procedure

Resolution	19.600 - 2.050
R-factor	0.2568
Rwork	0.255
R-free	0.27950
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	6m4r
Refinement software	PHENIX (1.18.2_3874)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	19.780	2.110
High resolution limit [Å]	2.050	2.050
Rmerge	0.099	0.511
Number of reflections	30333	2522
<I/σ(I)>	7
Completeness [%]	88.8
Redundancy	2.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		298	PEG