7F9F
Thrombocorticin
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 21-ID-F |
| Synchrotron site | APS |
| Beamline | 21-ID-F |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2015-06-22 |
| Detector | RAYONIX MX300HE |
| Wavelength(s) | 0.97892 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 42.458, 92.445, 58.536 |
| Unit cell angles | 90.00, 102.76, 90.00 |
Refinement procedure
| Resolution | 30.474 - 1.411 |
| R-factor | 0.17 |
| Rwork | 0.169 |
| R-free | 0.19370 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 7f91 |
| RMSD bond length | 0.005 |
| RMSD bond angle | 0.882 |
| Data scaling software | HKL-2000 |
| Phasing software | PHASER |
| Refinement software | PHENIX ((1.14_3260: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 1.430 |
| High resolution limit [Å] | 1.410 | 1.410 |
| Number of reflections | 84334 | 4206 |
| <I/σ(I)> | 25.2 | |
| Completeness [%] | 99.9 | |
| Redundancy | 5.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 293 | MgCl2, Tris, PEG 4000 |
