Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 123.15 |
Detector technology | CCD |
Collection date | 2014-12-28 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9792 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 308.956, 106.663, 198.708 |
Unit cell angles | 90.00, 125.96, 90.00 |
Refinement procedure
Resolution | 33.877 - 3.366 |
R-factor | 0.2579 |
Rwork | 0.256 |
R-free | 0.29390 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2r5k |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.15.2_3472) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.420 |
High resolution limit [Å] | 3.360 | 3.360 |
Number of reflections | 70378 | 6595 |
<I/σ(I)> | 10.8 | |
Completeness [%] | 95.2 | |
Redundancy | 2.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293.15 | 0.1M Succinic acid pH 5.5, 9.5% PEG 3350 |