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7F8F

Roadblock from Odinarchaeota LCB_4

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsNSRRC BEAMLINE TPS 05A
Synchrotron siteNSRRC
BeamlineTPS 05A
Temperature [K]100
Detector technologyCCD
Collection date2018-10-10
DetectorRAYONIX MX-300
Wavelength(s)1
Spacegroup nameI 21 21 21
Unit cell lengths52.072, 59.245, 59.890
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution39.300 - 1.830
Rwork0.193
R-free0.21600
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3l7h
RMSD bond length0.002
RMSD bond angle0.448
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwareACORN
Refinement softwarePHENIX (v1.17.1)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]42.1001.870
High resolution limit [Å]1.8301.830
Rmerge0.0460.524
Rmeas0.0500.566
Rpim0.0190.211
Number of reflections8418813
<I/σ(I)>18.52.6
Completeness [%]99.8
Redundancy7.1
CC(1/2)0.889
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION293200 mM MgSO4 20% PEG 4000 10% glycerol

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